驱蚊酯的合成及应用研究

本文合成了一种高效低毒驱蚊剂-驱蚊酯[(insectifuge ester)[1],3-(Acetyl-butyl-amino)-propionic acid ethyl ester],并对其结构进行了全面鉴定,同时对其合成过程中所产生的副产物进行了分析测定。用驱蚊酯配成含2.3%驱蚊酯的花露水,并测试了其驱蚊效果,有效驱蚊时间可达5小时以上。     

Fabrication of Fe-, Ni- and FeNi-coated Al2O3 core-shell microspheres by heterogeneous precipitation

The precursors with NiCO₃·2Ni(OH)₂·2H₂O-, Fe₂O₃·nH₂O-, or both of NiCO₃·2Ni(OH)₂·2H₂O- and Fe₂O₃·nH₂O-coated alumina microspheres were prepared, respectively, by the aqueous heterogeneous precipitation using metal salts, ammonium hydro-carbonate and -Al₂O₃ micropowders as the starting materials. Subsequently, magnetic metallic Ni-, -Fe- and γ-FeNi-coated alumina core-shell structural microspheres were successfully obtained by thermal reduction of the as-prepared precursors at 700 °C for 2 h, respectively. Optimized precipitation processing parameters of the concentration of alumina micropowders (15 g/L), the rate of adding reactants (5 mL/min) and pH value were determined by a trial and error method. Powders of the precursors and the resultant metal (Ni, -Fe, γ-FeNi alloy)-coated alumina micropowders were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The experimental results show that it is possible to adjust metal coating thicknesses and fabricate multilayer structured metal/ceramics core-shell microspherical powder materials and these materials may be applied for high performance of functional materials and devices.     

用摄动—加权残数法分析复合材料层合薄板的大挠度问题

本文将摄动法与加权残数法联合应用于解复合材料层合薄板的大挠度问题,对摄动后得到的各线线性微分方程组,全部采用统一试函数形式的最小二乘配点法求解,方法简捷,程序通用。     

ESA多功能测试仪的设计与实现

本文以引信电子安全系统(ESA)为应用背景,应用美国ADI公司生产的新型单片机ADμ C812,设计并实现了为ESA模拟产生各种环境信号,并能够同时对ESA的工作状态进行实时检测的一款实用设备--多功能测试仪,为ESA的进一步研制和开发应用奠定了一定的基础.     

iShopFloor: an Internet-enabled agent-based intelligent shop floor

Global competition is driving manufacturing companies to change the way they do business. New kinds of shop floor control systems need to be implemented for these companies to respond quickly to changing shop floor environments and customer demands. This paper presents a new concept called iShopFloor-an intelligent shop floor based on the Internet, web, and agent technologies. It focuses on the implementation of distributed intelligence in the manufacturing shop floor. The proposed approach provides the framework for components of a complex control system to work together as a whole rather than as a disjoint set. It encompasses both information architecture and integration methodologies. The paper introduces the basic concept of iShopFloor, a generic system architecture, and system components. It also describes the implementation of eXtensible Markup Language message services in iShopFloor and the application of intelligent agents to distributed manufacturing scheduling. A prototype environment is presented, and some implementation issues are discussed.     

Evaluating the mixing performance of a ribbon blender

This paper investigates the effects of processing and equipment parameters of a ribbon blender (i.e. loading method of lubricant, fill level, blade speed and blade design) on magnesium stearate homogeneity. A core sampling technique is used to obtain at least one hundred samples per sampling event, which are extracted throughout the blender and yield a thorough characterization of the entire bed. The results presented here can be used as a guideline to develop appropriate blending processes and characterization protocols for ribbon blenders.     

大孔径石蜡加氢精制催化剂的制备

采用氨吸附-程序升温脱附(NH3-TPD)、低温N2吸附(BET)、压汞法以及加氢精制活性评价等技术,探索SiO2-Al2O3载体在制备过程中孔结构和表面性质的变化。实验结果表明,采用特殊扩孔剂制备载体,当焙烧温度为700℃时,平均孔径可达到17.3nm,其中孔径大于20nm的孔占总孔体积的13.2%;同时载体表面上的中、强酸中心也全部丧失,均为弱酸中心。采用该载体制备的MoNiP/SiO2-Al2O3石蜡加氢精制催化剂,在MoO3用量减少了约1/4的情况下,比目前工业上使用的催化剂具有更高的脱金属能力和加氢精制活性。